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Saturday, April 13, 2013

Determination of Copper by Complexation, Solvent–Extraction and Spectrophotometry


Determination of Copper by Complexation, Solvent-Extraction and Spectrophotometry


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Abstract

To determine the concentration of squealer in an unnoticeable solution by using copper complexation, solvent stock and spectrophotometry. Standards atomic number 18 used to create a calibration booze-up and the unknown concentration of copper is then calculated by using the linear equation from the calibration curve. The concentration of copper in the unknown solution 201 was found to be 12.57± 0.25 ?g/mL.

Introduction

Copper is an essential mineral in everyday life, it is in necessary for the production of vehement blood and it also keeps the immune systems, nervous system ad hones healthy.[7] Too much copper in a fast can possible health risks. There are some(prenominal) different ways to determine the concentration of copper in the unknown solution such as colourimetric titration, microwave digestions and spectrophotometry up to now using the solvent-extraction provides the virtually accurate measurements of solvent and using the spectrophotometry provides frank accuracy at low concentrations of 10-6 g/m (ppm).

Theory

Solvent Extraction is the transfer of a solute from one form to an some other.

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This process allows to isolate or cut down the desired analyte or to separate it from species that would interfere in the analysis. The most used process is the extraction of an aqueous solution with an organic solvent. Diethylether, toluene, and hexane are common solvents that are immiscible with and less large(p) than water. They form a separate phase that ?oats on return of the aqueous phase. Chloroform and carbon tetrachloride are common solvents that are denser than water. In the two-phase mixture, one phase is mostly water and the other phase is mostly organic because they are immiscible liquids. two liquids are miscible if they form a single phase when they are mixed in any...

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